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CRYSTAL DEFECTS AND GRAIN INTERFACE STRUCTURE OF ION-NITRIDED LAYERS

SUN Dongsheng LI Fengzhao Shandong Polytechnic University , Jinan , Laboratory of Atomic Imaging of Solids , Institute of Metal Research , Academia Sinica , Shenyang , ChinaDAI Jiyan LI Douxing Laboratory of Atomic Imaging of Solids , Institute of Metal Research , Academia Sinica , Shenyang , China associate professor , Institute of Materials Engineering , Shandong Polytechnic University , Jinan 250014 , China

金属学报(英文版)

Observation under high resolution electron microscope shows that the continuous bombing of high speed ions produces a great amount of vacant site defects.The assembly of vacancies forms vacant dish,and the collapase of vacant dish forms stacking fault tetrahedrons and oth- er crystal defects.The interfaces between phase ε(Fe_(2-3)N)and phase γ'(Fe_4N)are smooth, straight and coherent,and they have the orientation relationships of(11)//(0001)and [110]/[110] .

关键词: crystal defect , null , null , null

FACTORS AFFECTING SILICA CONTENT OF ALUMINIUM HYDROXIDE PRODUCT IN CARBONIZATION PROCESS

LIU Miaoxiu CHENG Zhaonian CHEN Nianyi Shanghai Institute of Metallurgy , Academia Sinica , Shanghai , ChinaKE Jiajun Institute of Chemical Metallurgy , Academia Sinica , Beijing , China CHEN Nianyi , Professor , Shanghai Institute of Metallurgy , Academia Sinica , Shanghai 200050 , China

金属学报(英文版)

The regularity of the carbonization process in alumina production has been summarized by the pattern recognition and regression.A mathematical model has been proposed to describe the factors affecting the silica content of aluminium hydroxide product.The high concentration of aluminate ions in solution will produce aluminium hydroxide with low content of SiO_2 under the condition of Al_2O_3/SiO_2 ratio kept unchanged.This was confirmed by certain scale experiments.

关键词: carbonization , null , null , null

INFLUENCE OF BORON ON MICROSTRUCTURE AND MECHANICAL PROPERTIES OF RAPIDLY SOLIDIFIED Ni_3Al

LI Hui Institute of Metal Research , Academia Sinica , Shenyang , ChinaLIU Xiang Northeast Institute of Technology , Shenyang , ChinaGUO Jianting HU Zhuangqi Institute of Metal Research , Academia Sinica , Shenyang , China Associate Professor , Institute of Metall Research , Academia Sinica , Shenyang , China

金属学报(英文版)

By means of nonstoichiometry,rapid solidification and adequate boron addition,the tensile strength and bending resistance of Ni_3Al has been improved.When adding 0.52 to 1.37 at.-% B into Ni_3Al,which has the beneficial effect on the ductility.If boron addition is too high, there are coarse Ni_(23)B_6 particles and NiB_(12) phases found at the grain boundaries.Boron modification in Ni_3Al promotes the ordering in the region near grain boundaries.The grain boundary of boron free Ni_3Al is a large angle one,but turns into a small angle grain bound- ary with sub-grains of dislocation characteristics when the boron content in Ni_3Al reaches 1.37 at.-%.

关键词: intermetallic compound , null , null , null

STRUCTURE AND SURFACE CONDITION OF ULTRAFINE AI PARTICLES

SUN Xiukui CHEN Wenxiu XU Jian FAN Xueshu WEI Wenduo State Key Laboratory of Rapidly Solidified Non-Equilibrium Alloys , Institute of Metal Research , Academia Sinica , Shenyang , ChinaWU Yukun PENG Yingguo Laboratory of Atomic Imaging of Solids , Institute of Metal Research , Academia Sinica , Shenyang , China Associate Professor , Institute of Metal Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The crystal habit,crystalline structure,surface condition and composition of the ultrafine Al particles prepared by inert gas evaporation method were studied in detail by means of high resolution transmission electron microscope,X-ray diffraction and X-ray photo-electron spectrum.The results indicate that the ultrafine Al particles prepared in high pure inert gas are of clear crystal habits,single crystal in a large majority and fcc crystalline structure with a_0=0.405 nm.It is also found on the surface of the Al particles that there is a layer of amor- phous Al_2O_3 with 2 nm average thickness,which could protect the particles against oxidizing further.Therefore,the ultrafine Al particles prepared by the inert gas evaporation method are very stable in atmosphere.

关键词: ultrafine Al particle , null , null , null

EFFECT OF SLIP ORIENTATION ON STRESS RESPONSE,INTERNAL FRICTION AND ULTRASONIC ATTENUATION DURING CYCLIC DEFORMATION IN Al SINGLE CRYSTALS

XIA Yuebo ZHANG Tianyi State Key Laboratory for Fatigue and Fracture of Materials , Institute of Metal Research , Academia Sinica , Shenyang , ChinaFEI Guangtao ZHOU Xing Laboratory of Internal Friction and Defects in Solids , Institute of Solid State Physics , Academia Sinica , Hefei , China Associate Professor , Institute of Metal Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The variation of cyclic stress,internal friction and ultrasonic attenuation during cyclic deformation and relations among them have been investigated with different slip orientation Al single crystals.The results indicate that the value of cyclic stress σ,internal friction Q~(-1)and ultrasonic attenuation △α depend obviously on the slip orientation.There are large differences in above three parameters for different slip orientation Al crystals.In early stage of fatigue life,σ and △α increase and Q~(-1)decreases with cycles N,and △α reached maxi- mum before σ,while Q~(-1)and σ get the valley and the peak,respectively,at same cycles.

关键词: crystal orientation , null , null , null , null , null

END GRAIN ATTACK OF LD10CS PLATES DURING CHEMICAL MILLING

ZENG Xianghua , SHA Jiande , SU Ge Institute of Metal Research , Academia Sinica , Shenyang , ChinaYUAN Jigang LIU Fumei ZHONG Huiwen Southwest Aluminium Mill , China National Nonferrous Metals Industry Corporation , Chongqing , China SHA Jiande , Engineer , Institute of Metal Research , Academia Sinica , Shenyang , China

金属学报(英文版)

The end grain attack of LDIOCS aluminium alloy plates during chemical milling in hot aqueous solution of sodium hydroxide has been studied.The results show that the microsegregation of some components,i.e.Cu,Si etc.,is the main reason of the end grain at- tack,and it is affected by the conditions of heat treatment as well.The end grain attack significantly diminishes while some technical measures which are beneficial to the reduce of segregation were taken during melting and casting.

关键词: aluminium alloy , null , null , null

TENSILE AND ADHESIVE STRENGTHS OF FINE TiN FILM ON Ti SUBSTRATE

LIU Changqing , LI Meishuan , JIN Zhujing , WU Weitao Corrosion Science Laboratory , Institute of Corrosion and Protection of Metals , Academia Sinica , Shenyang , China research assistant , Institute of Corrosion and Protection of Metals , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The cantilever bending test,particularly monitored by an acoustic emission technique, was adopted to measure the tensile and interfacial adhesive strengths of the HCD ion plated fine TiN film on pure Ti substrate.The behaviors of film damaging were found to be characterized by:an internal tensile stress which exceeded its tensile strength for TiN facing upward,and a shearing stress along film substrate interface which exceeded its adhesive strength for TiN facing downward.The measured tensile and adhcsive strengths are 603 and 242 MPa respectively.

关键词: tensile strength , null , null , null

AN EXPERT SYSTEM FOR COMPUTER AIDED ALLOY STEEL DESIGN—ASPRES

CHEN Yu , CHEN Nianyi Shanghai institute of Metallurgy , Academia Sinica , Shanghai , China PENG Ping , KONG Bingyu Iron and Steel Research Institute , Shanghai Baoshan Iron and Steel Complex , Shanghai , China professor , Shanghai Institute of Metallurgy , Academia Sinica , Shanghai 200050 , China

金属学报(英文版)

An alloy steel pattern recognition expert system,ASPRES,has been established for the purpose of computer aided optimal design of alloy steel in compositions and process pa- rameters,Pattern recognition techniques are used to abstract inner relationship between mechanical properties and process variables.The ASPRES uses 2-dimensional graph as visual knowledge to represent domain expertise of specific object.Forward and back- ward chaining can be utilized by researcher in predicting sample performances or giving helpful suggestions about the chemical compositions and process parameters according to desired properties.

关键词: pattern recognition , null , null

BEHAVIOURS OF AUSTEN1TE UNDER IMPACT ABRASION

WANG Huaming Institute of Metal Research , Academia Sinica , Shenyang , ChinaZHANG Qing Central Iron and Steel Research Institute , Ministry of Metallurgical Industry , Beijing , ChinaSHAO Hesheng Beijing Graduate School , China University of Mining and Technology , Beijing , China Institute of Metal Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The role of austenite in impact-abrasion process was studied on the basis of the impact-abrasion test results of a newly developed austenite-bainitic ferrite dual-phase abrasion-resistant steel with high strength,high toughness and high strain-hardening ability. It is found that the morphology,distribution and mechanical stability,rather than the volume fraction,of austenite govern the impact abrasion behaviour.Only the appropriate amount of fine and evenly dispersed austenite with adequate mechanical stability in high strength matrices,contribute effectively to the irnpact-abrasion resistance of the materials.While large quantity of coarse austenite with poor mechanical stability,especially when it acted as a continuous matrix of the material,is extremely detrimental to impact-abrasion resistance.

关键词: austenite , null , null , null

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